HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86735978, compound → HCID 70596492, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86735978 | HCID 86735978 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70596492 | HCID 70596492 | — |
Reaction Steps
A solution of 2.77 g of 1-pyrrolidino-3-p-biphenylyl-1-butene (obtainable from 3-p-biphenylyl-butanal and pyrrolidine) in 35 ml of ethanol is hydrogenated, over 0.5 g of Raney nickel, for 3 hours at 6 atms and 60°. The catalyst is filtered off and the solution is evaporated to give 1-pyrrolidino-3-p-biphenylyl-butane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04110447 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-f915f385dae5463b9c148743804d326b |
| Source note | uspto-grants-1978_08 |