Glycine → Trehalose glycine

HRID 2420664Notes

Reaction equation

HRID 2420664 reaction equation
[CH2:1]([OH:23])[C@H:2]1[O:7][C@H:6]([O:8][C@H:9]2[O:14][C@H:13]([CH2:15][OH:16])[C@@H:12]([OH:17])[C@H:11]([OH:18])[C@H:10]2[OH:19])[C@H:5]([OH:20])[C@@H:4]([OH:21])[C@@H:3]1[OH:22].O.O.[NH2:26][CH2:27][C:28]([OH:30])=[O:29]>O>[CH2:15]([OH:16])[C@H:13]1[O:14][C@H:9]([O:8][C@H:6]2[O:7][C@H:2]([CH2:1][OH:23])[C@@H:3]([OH:22])[C@H:4]([OH:21])[C@H:5]2[OH:20])[C@H:10]([OH:19])[C@@H:11]([OH:18])[C@@H:12]1[OH:17].[NH2:26][CH2:27][C:28]([OH:30])=[O:29]

Participants

5

Reactant 3

HCID 750GlycineHCID 181978Trehalose, dihydrateHCID 178435178HCID 178435178, compound

Product 1

HCID 69122788Trehalose glycine

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

17.84 g of trehalose dihydrate and 4.03 g of glycine were carefully weighed and transferred into a sterile polypropylene bottle, to which 300 ml of purified water was added at room temperature and stirred slowly until a clear solution was obtained. The pH was measured and found to be 5.5. Without adding any acid, the volume was adjusted to 350 ml with purified water. The pH was measured and found to be 5.5.

Workup

  1. additionwas added at room temperature
  2. customwas obtained
  3. additionWithout adding any acid

Sources & evidence

ORD record
ord-98c3198f70774fed8176f88e3b49eb54
Source dataset
uspto-grants-2011_06
Patent number
US07956028B2

Reaction notes

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