1,2-Dibromoethane → HCID 67214514, compound

HRID 2420717Notes

Reaction equation

HRID 2420717 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([C:7]([NH:9][C:10]2[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[C:12]([O:18][CH3:19])[CH:11]=2)=[O:8])[NH:5][CH:6]=1.Br[CH2:21][CH2:22]Br>>[Br:1][C:2]1[CH:3]=[C:4]2[C:7](=[O:8])[N:9]([C:10]3[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[C:12]([O:18][CH3:19])[CH:11]=3)[CH2:22][CH2:21][N:5]2[CH:6]=1

Participants

3

Reactant 2

HCID 78391,2-DibromoethaneHCID 17457221HCID 17457221, compound

Product 1

HCID 67214514HCID 67214514, compound

Procedure

Following the procedure described in Example 1 step D, the product of step A (140 mg) was alkylated with 1,2-dibromoethane to yield 143 mg of the title compound. MS (ESI) 351, 353 (M+H)+.

Sources & evidence

ORD record
ord-7b97580176634f18a5e29dea9a5d8560
Source dataset
uspto-grants-2011_06
Patent number
US07956049B2

Reaction notes

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