Malononitrile → HCID 57662879, compound
Reaction equation
[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[C:4]([O:10][CH3:11])[CH:3]=1.[C:12](#[N:16])[CH2:13][C:14]#[N:15]>>[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[C:13]([C:12]#[N:16])[C:14]#[N:15])=[C:4]([O:10][CH3:11])[CH:3]=1Participants
3
Procedure
By the method used for Intermediate 3,4-chloro-2-methoxybenzaldehyde from Step A was reacted with malononitrile to afford the title compound as a yellow solid. LC-MS 219 (M+1).
Sources & evidence
- ORD record
- ord-9c62db46700c47b498d1bcd9a1554e1a
- Source dataset
- uspto-grants-2011_06
- Patent number
- US07956061B2
Reaction notes
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