HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67215250, compound → HCID 67215270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67215250 | HCID 67215250 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67215270 | HCID 67215270 | 34.9% |
Reaction Steps
Benzyl 2-oxo-4-(2,2,2-trifluoroethyl)-2,3-dihydro-1,3-thiazole-5-carboxylate (0.6 g) in ethanol was treated with 5% palladium on carbon and hydrogenated at 3 bar for 8 days. After filtration, the solvent was evaporated to yield the title compound as a colourless oil (0.15 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07956070B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-b2778bbdd9084983b5c4d3ea64176081 |
| Source note | uspto-grants-2011_06 |