HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dimethoxybenzoic acid → HCID 16722538, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dimethoxybenzoic acid | HCID 7052 | — |
| Reactant | 5-Methyl-3-phenyl-4-isoxazolecarbohydrazide | HCID 727924 | — |
| Product | HCID 16722538 | HCID 16722538 | 62% |
Reaction Steps
As described for example 2, 5-methyl-3-phenyl-isoxazole-4-carboxylic acid hydrazide (200 mg, 0.92 mmol) was converted using 2,4-dimethoxybenzoic acid instead of o-toluic acid to the title compound (SiO2, heptane:ethyl acetate=80:20 to 50:50, 207 mg, 62%) which was obtained as a white solid. MS: m/e=364.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07956074B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-ac569529bb4146c1ac94f24e74e6670f |
| Source note | uspto-grants-2011_06 |