HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methyl-3-phenyl-4-isoxazolecarbohydrazide → HCID 16722908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methyl-3-phenyl-4-isoxazolecarbohydrazide | HCID 727924 | — |
| Reactant | 1,4-Benzenedicarboxylic acid, methyl ester | HCID 3614454 | — |
| Product | HCID 16722908 | HCID 16722908 | 60% |
Reaction Steps
As described for example 2, 5-methyl-3-phenyl-isoxazole-4-carboxylic acid hydrazide (2.00 g, 9.21 mmol) was converted using mono-methyl terephthalate instead of o-toluic acid to the title compound (1.98 mg, 60%) which was obtained as a colorless liquid. MS: m/e=310.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07956074B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-7244baf948144b6c81187fca401a4a81 |
| Source note | uspto-grants-2011_06 |