Phenethylamine → HCID 67214542, compound

Participants

Reaction Steps

Using preparation method 1, 96B (288 mg, 1.5 mmol) was reacted with phenethyl amine (276 μL, 266 mg, 2.2 mmol). Purification by flash chromatography on SiO2 using CH2Cl2/hexanes 50:50 then CH2Cl2 100% afforded white crystals (330 mg, 74%). NMR 1H (ppm, CDCl3): 7.52 (s, 1H), 7.44-7.41 (m, 1H), 7.34-7.22 (m, 7H), 6.09 (br. s, 1H), 3.74-3.67 (m, 2H), 2.92 (t, J3=6.9 Hz, 2H), 2.64-2.59 (m, 2H), 1.63-1.40 (m, 3H), 0.92 (d, J3=6.3 Hz, 6H).

Provenance & Evidence