HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Methylphenyl)hydrazine → 3-[(2-fluoro-4-iodophenyl)amino]-N'-(4-methylphenyl)isonicotinohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Methylphenyl)hydrazine | HCID 10875 | — |
| Reactant | 3-((2-Fluoro-4-iodophenyl)amino)isonicotinic acid | HCID 59026791 | — |
| Product | 3-[(2-fluoro-4-iodophenyl)amino]-N'-(4-methylphenyl)isonicotinohydrazide | HCID 11532734 | — |
Reaction Steps
3-[(2-fluoro-4-iodophenyl)amino]-N′-(4-methylphenyl)isonicotinohydrazide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.4 mmol of 3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid (intermediate 1) and 0.6 mmol of 4-methyl-phenylhydrazine. LC/MS [5.07 min; 463 (M+1)]
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07956191B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-8535d3f6ab784321bb6e048eb2506df9 |
| Source note | uspto-grants-2011_06 |