HCID 86629175, compound → HCID 86629174, compound

Participants

Reaction Steps

810 mg of 38 (1.936 mmol), 69.84 mg of Pd/C (10%) and 20 mL of MeOH are hydrogenated at 5 bar for 10 hours at 20° C. in an autoclave. After filtering off the catalyst through Celite, the solvent is evaporated off and 580 mg of expected product 39 are obtained, which product is used directly in the following step.

Provenance & Evidence