HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86629181, compound → HCID 86629180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86629181 | HCID 86629181 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86629180 | HCID 86629180 | 92.5% |
Reaction Steps
790 mg of 48 (2.192 mmol), 79 mg of Pd/C (10%) and 20 mL of ethanol are hydrogenated at 7 bar for 10 hours at 20° C. in an autoclave. After filtering off the catalyst through Celite, the solvent is evaporated off and 670 mg of expected product 49 are obtained (yellow oil), which product is used directly in the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960373B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-7d58dbdf4d0040db9b26fe19eff9152e |
| Source note | uspto-grants-2011_06 |