HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethyl)phenyl isocyanate → HCID 58834853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethyl)phenyl isocyanate | HCID 9483 | — |
| Reactant | 1-(4-Fluorophenyl)piperazine | HCID 75260 | — |
| Reactant | HCID 11826263 | HCID 11826263 | — |
| Product | HCID 58834853 | HCID 58834853 | — |
Reaction Steps
Starting with 5.0 g (11.43 mmol) of the iminophosphorane from Example 3A, 2.25 g (12.0 mmol) of trifluoro-m-tolyl isocyanate and 2.06 g (11.43 mmol) of N-(4-fluorophenyl)piperazine, the general procedure [E] gives 3.31 g (39% of theory) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960387B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-b789c15cd7e14ebeb7185e3b1b1019d0 |
| Source note | uspto-grants-2011_06 |