HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoic Acid → N-(3-methoxyphenyl)-4-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoic Acid | HCID 6108 | — |
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Product | N-(3-methoxyphenyl)-4-nitrobenzamide | HCID 774514 | 93.2% |
Reaction Steps
Using m-anisidine (2.50 g, 15.0 mmol) and 4-nitrobenzoic acid (2.03 g, 16.5 mmol), the procedure of Reference Example 16 was repeated to obtain 3.80 g (93.2%) of the title compound in the form of light yellow needle crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-b82805e2b34b4ecf82e3f2502d0befca |
| Source note | uspto-grants-1998_03 |