Benzo-1,3-dioxole-5-methylamine → HCID 11697355, compound

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Reaction Steps

The title compound was prepared from 4-chloro-2-(2-methoxyethyl)-5-phenylisothiazol-3(2H)-one 1,1-dioxide and 1-(1,3-benzodioxol-5-yl)methanamine in a similar manner as described for Example 1. 1H NMR (400 MHz, CD3CN): δ 7.32-7.49 (m, 5H), 6.64 (d, 1H), 6.31-6.38 (m, 2H), 6.25-6.29 (m, 1H), 5.91 (s, 2H), 4.05 (d, 2H), 3.83 (t, 2H), 3.67 (t, 2H), 3.35 (s, 3H); Mass Spectrum: M−H+ 415.

Provenance & Evidence