HCID 57542014, compound → HCID 57541912, compound

Participants

Reaction Steps

To a solution of methyl 4-[[3-((E)-2-phenylethenyl) phenyl]methoxy]benzenepropanoate (0.35 g, 0.95 mmol) in methanol (15 mL) and tetrahydrofuran (25 mL) was added platinum oxide (0.018 g, 0.078 mmol), and the mixture was stirred under a hydrogen atmosphere at room temperature for 18 hrs. The catalyst was filtered off, and the filtrate was concentrated. The residue was purified by silica gel column chromatography (ethyl acetate/hexane=15:1) to give the title compound (0.21 g, yield 58%). oil.

Provenance & Evidence