HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 51458-31-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 15480691 | HCID 15480691 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 51458-31-2 | HCID 12112424 | 79% |
Reaction Steps
A mixture of tert-butyl (2E)-3-[4-(benzyloxy)phenyl]acrylate (13.3 g, 42.8 mmol), 10% Pd carbon (1.3 g), ethanol (100 mL) and tetrahydrofuran (30 mL) was stirred under a hydrogen atmosphere for 2 hrs. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure to give the title compound (7.5 g, yield 79%) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960369B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-b4396e01e13f457b93c717e31eb81cde |
| Source note | uspto-grants-2011_06 |