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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2422262Generated: October 31, 2026

Ethanol → 51458-31-2

https://huagongshe.com/reaction/2422262

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantHCID 15480691HCID 15480691—
CatalystHCID 178418390HCID 178418390—
SolventTetrahydrofuranHCID 8028—
Product51458-31-2HCID 1211242479%

Reaction Steps

A mixture of tert-butyl (2E)-3-[4-(benzyloxy)phenyl]acrylate (13.3 g, 42.8 mmol), 10% Pd carbon (1.3 g), ethanol (100 mL) and tetrahydrofuran (30 mL) was stirred under a hydrogen atmosphere for 2 hrs. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure to give the title compound (7.5 g, yield 79%) as colorless crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07960369B2
Source datasetuspto-grants-2011_06
ORD IDord-b4396e01e13f457b93c717e31eb81cde
Source noteuspto-grants-2011_06