Benzenepropanoic acid, 4-hydroxy-, methyl ester → HCID 57542024, compound

HRID 2422277Notes

Reaction equation

HRID 2422277 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][C:10]([O:12]C)=[O:11])=[CH:4][CH:3]=1.[CH2:14]([C:18]1[CH:23]=[CH:22][CH:21]=[C:20]([CH3:24])[C:19]=1[C:25]1[CH:30]=[CH:29][CH:28]=[C:27]([CH2:31]O)[CH:26]=1)[CH:15]([CH3:17])[CH3:16]>>[CH2:14]([C:18]1[CH:23]=[CH:22][CH:21]=[C:20]([CH3:24])[C:19]=1[C:25]1[CH:30]=[CH:29][CH:28]=[C:27]([CH2:31][O:1][C:2]2[CH:3]=[CH:4][C:5]([CH2:8][CH2:9][C:10]([OH:12])=[O:11])=[CH:6][CH:7]=2)[CH:26]=1)[CH:15]([CH3:17])[CH3:16]

Participants

3

Reactant 2

HCID 79706Benzenepropanoic acid, 4-hydroxy-, methyl esterHCID 23083108HCID 23083108, compound

Product 1

HCID 57542024HCID 57542024, compound

Procedure

The title compound was synthesized in the same manner as in Reference Example 230 from methyl 3-(4-hydroxyphenyl)propanoate and (2′-isobutyl-6′-methylbiphenyl-3-yl)methanol. colorless oil (yield 58%). MS (APCI−): 401 (M−H).

Sources & evidence

ORD record
ord-b847a84cb252472ca0e43ee972452dc2
Source dataset
uspto-grants-2011_06
Patent number
US07960369B2

Reaction notes

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