Benzenepropanoic acid, 4-hydroxy-, methyl ester → HCID 57542034, compound

HRID 2422278Notes

Reaction equation

HRID 2422278 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][C:10]([O:12]C)=[O:11])=[CH:4][CH:3]=1.[CH2:14]([C:16]1[CH:21]=[CH:20][CH:19]=[C:18]([CH3:22])[C:17]=1[C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([CH2:29]O)[CH:24]=1)[CH3:15]>>[CH2:14]([C:16]1[CH:21]=[CH:20][CH:19]=[C:18]([CH3:22])[C:17]=1[C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([CH2:29][O:1][C:2]2[CH:3]=[CH:4][C:5]([CH2:8][CH2:9][C:10]([OH:12])=[O:11])=[CH:6][CH:7]=2)[CH:24]=1)[CH3:15]

Participants

3

Reactant 2

HCID 79706Benzenepropanoic acid, 4-hydroxy-, methyl esterHCID 23083012HCID 23083012, compound

Product 1

HCID 57542034HCID 57542034, compound

Procedure

The title compound was synthesized in the same manner as in Reference Example 230 from methyl 3-(4-hydroxyphenyl)propanoate and (2′-ethyl-6′-methylbiphenyl-3-yl)methanol. colorless crystals (yield 57%). MS (APCI−): 373 (M−H).

Sources & evidence

ORD record
ord-a076fc53662742d7b3b5be06fcbdf47b
Source dataset
uspto-grants-2011_06
Patent number
US07960369B2

Reaction notes

Loading…