2-Cyanophenylboronic acid → HCID 23083138, compound

HRID 2422289Notes

Reaction equation

HRID 2422289 reaction equation
Br[C:2]1[CH:3]=[C:4]([CH:19]=[CH:20][CH:21]=1)[CH2:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([CH2:13][CH2:14][C:15]([O:17]C)=[O:16])=[CH:9][CH:8]=1.[C:22]([C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=1B(O)O)#[N:23]>>[C:22]([C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=1[C:2]1[CH:21]=[CH:20][CH:19]=[C:4]([CH2:5][O:6][C:7]2[CH:12]=[CH:11][C:10]([CH2:13][CH2:14][C:15]([OH:17])=[O:16])=[CH:9][CH:8]=2)[CH:3]=1)#[N:23]

Participants

3

Reactant 2

HCID 27346102-Cyanophenylboronic acidHCID 23136270Methyl 4-[(3-bromophenyl)methoxy]benzenepropanoate

Product 1

HCID 23083138HCID 23083138, compound

Procedure

The title compound was synthesized in the same manner as in Example 272 from methyl 3-[4-[(3-bromobenzyl)oxy]phenyl]propanoate and 2-cyanophenylboronic acid. colorless crystals (yield 6%). MS (APCI−): 356 (M−H).

Sources & evidence

ORD record
ord-8b8cd2c5ba7141a5ac89a358b06e1d00
Source dataset
uspto-grants-2011_06
Patent number
US07960369B2

Reaction notes

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