2-Ethoxycarbonylphenylboronic acid → HCID 23082909, compound
Reaction equation
Br[C:2]1[CH:3]=[C:4]([CH:19]=[CH:20][CH:21]=1)[CH2:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([CH2:13][CH2:14][C:15]([O:17]C)=[O:16])=[CH:9][CH:8]=1.[CH2:22]([O:24][C:25]([C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=1B(O)O)=[O:26])[CH3:23]>>[CH2:22]([O:24][C:25]([C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=1[C:2]1[CH:21]=[CH:20][CH:19]=[C:4]([CH2:5][O:6][C:7]2[CH:12]=[CH:11][C:10]([CH2:13][CH2:14][C:15]([OH:17])=[O:16])=[CH:9][CH:8]=2)[CH:3]=1)=[O:26])[CH3:23]Participants
3
Procedure
The title compound was synthesized in the same manner as in Example 272 from methyl 3-[4-[(3-bromobenzyl)oxy]phenyl]propanoate and 2-ethoxycarbonylphenylboronic acid. colorless oil (yield 12%).
Sources & evidence
- ORD record
- ord-73f71e403e81492d83dead3883218160
- Source dataset
- uspto-grants-2011_06
- Patent number
- US07960369B2
Reaction notes
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