HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilic Acid → HCID 11618024, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilic Acid | HCID 227 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Cyclobutanone | HCID 14496 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | Tert-butyl 4-hydroxypiperidine-1-carboxylate | HCID 643502 | — |
| Product | HCID 11618024 | HCID 11618024 | — |
Reaction Steps
The entitled compound was obtained according to the method of Example 85 but using anthranilic acid, methylamine, 4-methoxybenzaldehyde, tert-butyl 4-hydroxytetrahydro-1(2H)-pyridinecarboxylate, and cyclobutanone. The obtained compound was further purified through reversed-phase high-performance liquid chromatography (acetonitrile-water) to give a colorless solid (m.p. 167.8-171.2° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960394B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-1a8efbf46c5841a7a115d78b190adbb7 |
| Source note | uspto-grants-2011_06 |