HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoic Acid → N-(2,5-Dimethoxyphenyl)-4-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoic Acid | HCID 6108 | — |
| Reactant | 2,5-Dimethoxyaniline | HCID 7613 | — |
| Product | N-(2,5-Dimethoxyphenyl)-4-nitrobenzamide | HCID 532160 | 77.2% |
Reaction Steps
Using 2,5-dimethoxyaniline (2.53 g, 16.5 mmol) and 4-nitrobenzoic acid (2.51 g, 15.0 mmol), the procedure of Reference Example 16 was repeated to obtain 3.50 g (77.2%) of the title compound in the form of orange needle crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-94cb357d0d594c1a9f47342a518b5646 |
| Source note | uspto-grants-1998_03 |