HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Difluoroaniline → N-(3,4-Difluorophenyl)-1H-benzimidazol-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Difluoroaniline | HCID 77469 | — |
| Reactant | 2-Chlorobenzimidazole | HCID 78572 | — |
| Product | N-(3,4-Difluorophenyl)-1H-benzimidazol-2-amine | HCID 15604436 | — |
Reaction Steps
The title compound was prepared from 2-chlorobenzimidazole and 3,4-difluoroaniline by Procedure A. The product was isolated by filtration to give the title compound as a hydrochloride salt (white solid, mp 283-284° C.). MS(ES+) m/z 246 ([M+1]+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960561B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-024fc23f32214056aa634a57aa7fd10a |
| Source note | uspto-grants-2011_06 |