HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxybenzyl alcohol → HCID 178439654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxybenzyl alcohol | HCID 102 | — |
| Reactant | 4-allyl-5-hydroxy-N-neopentylindole | HCID 18672464 | — |
| Reactant | 1-(2,2-dimethylpropyl)-4-propyl-5-{4-[4-(1H-tetrazol-5-yl)phenoxy]butoxy}-1H-indole | HCID 178439686 | — |
| Product | HCID 178439654 | HCID 178439654 | — |
Reaction Steps
A similar reaction sequence as outlined in example 28 was followed using 3-(hydroxymethyl)phenol and 4-allyl-1-(2,2-dimethylpropyl)-1H-indol-5-ol, an intermediate from example 1. 1H NMR (CDCl3, 500 MHz) δ 7.97 (d, 2H), 7.43 (t, 1H), 7.30 (d, 1H), 7.20 (br s, 1H), 7.16 (d, 1H), 7.10 (s, 1H), 7.08 (d, 2H), 7.04-7.06 (m, 1H), 6.93 (d, 1H), 6.5 (br s, 1H), 5.90-6.03 (m, 1H), 5.10 (s, 2H), 5.05 (d, 1H), 4.95 (d, 1H), 3.90 (d, 2H), 3.68 (d, 2H), 1.00 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960417B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-993ec59c510248d186556af28b69b5f5 |
| Source note | uspto-grants-2011_06 |