HCID 23087108, compound → HCID 57934534, compound

HRID 2423568Notes

Reaction equation

HRID 2423568 reaction equation
NC1(C[O:8]C2C=CC(C#N)=CC=2)CCCC1.[CH3:17][N:18]([CH3:34])[C:19]1([CH2:24][O:25][C:26]2[CH:33]=[CH:32][C:29]([C:30]#N)=[CH:28][CH:27]=2)[CH2:23][CH2:22][CH2:21][CH2:20]1>>[CH3:17][N:18]([CH3:34])[C:19]1([CH2:24][O:25][C:26]2[CH:33]=[CH:32][C:29]([CH:30]=[O:8])=[CH:28][CH:27]=2)[CH2:23][CH2:22][CH2:21][CH2:20]1

Participants

3

Reactant 2

HCID 23087108HCID 23087108, compoundHCID 23087111HCID 23087111, compound

Product 1

HCID 57934534HCID 57934534, compound

Procedure

Synthesized from 4-(1-aminocyclopentylmethoxy)benzonitrile according to an analogous synthetic method to Preparation Example 18, 4-(1-dimethylaminocyclopentylmethoxy)benzonitrile (1.2 g) was used according to an analogous synthetic method to Preparation Example 16 to provide the title compound (1.2 g).

Workup

  1. customwas used according to an analogous synthetic method to Preparation Example 16

Sources & evidence

ORD record
ord-6a5b26ff89bd421cacb662416ce7cf8f
Source dataset
uspto-grants-2011_06
Patent number
US07960412B2

Reaction notes

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