HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
7-Methoxy-2-tetralone → 6-Methoxy-3-(4-methoxy-2-nitrophenyl)-1,2-dihydronaphthalene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 7-Methoxy-2-tetralone | HCID 77785 | — |
| Edukt | 7-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate | HCID 23087446 | — |
| Edukt | Tributyl(4-methoxy-2-nitrophenyl)tin | HCID 23087474 | — |
| Produkt | 6-Methoxy-3-(4-methoxy-2-nitrophenyl)-1,2-dihydronaphthalene | HCID 23087535 | — |
Reaktionsschritte
Synthesized from 7-methoxy-2-tetralone according to an analogous synthetic method to Preparation Example 82 described above, 7-methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate (3.5 g) and tributyl(4-methoxy-2-nitrophenyl)tin (18 g) were used according to an analogous synthetic method to Preparation Example 77 to provide the title compound (1.9 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07960412B2 |
| Quelldatensatz | uspto-grants-2011_06 |
| ORD ID | ord-b9ebb95c7f274cb7a6fab4f86e5143c4 |
| Quellennotiz | uspto-grants-2011_06 |