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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2423623Generated: October 25, 2026

1-Bromo-4-fluoro-2-nitrobenzene → HCID 23087411, compound

https://huagongshe.com/reaction/2423623

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Bromo-4-fluoro-2-nitrobenzeneHCID 2773383—
Reactant6-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonateHCID 15330256—
ReactantTributyl(4-fluoro-2-nitrophenyl)tinHCID 23087155—
ProductHCID 23087411HCID 23087411—

Reaction Steps

Synthesized from 1-bromo-4-fluoro-2-nitrobenzene according to an analogous synthetic method to Preparation Example 76, tributyl(4-fluoro-2-nitrophenyl)tin (7.1 g) and 6-methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate (2.2 g) were used according to an analogous synthetic method to Preparation Example 77 to provide 3-(4-fluoro-2-nitrophenyl)-7-methoxy-1,2-dihydronaphthalene (1.4 g). The total amount of this compound was used according to an analogous synthetic method to Example 30 to provide the title compound (1.1 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07960412B2
Source datasetuspto-grants-2011_06
ORD IDord-df1c56a679074deba863db19228d68f9
Source noteuspto-grants-2011_06