HRID2423648

反应详情

EQUATION

反应方程式

HRID 2423648 的结构方程式

PROCEDURE

实验过程

Synthesized from 2-methoxy-5,7,8,9-tetrahydrobenzocyclohepten-6-one according to an analogous synthetic method to Preparation Example 82, 2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl trifluoromethanesulfonate (3.0 g) and tributyl(4-methoxy-2-nitrophenyl)tin (10.8 g) were used according to an analogous synthetic method to Preparation Example 77 to provide the title compound (2.8 g).

WORKUP

后处理

  1. customwere used according to an analogous synthetic method to Preparation Example 77