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HRID2423942

反应详情

EQUATION

反应方程式

HRID 2423942 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=O)CCl
HCID75886

2-Chloro-N,N-dimethylacetamide

C4H8ClNO

结构：COc1ccc(C2CCc3cc(OC(=O)C(C)(C)C)ccc3C2)c(N(C(=O)c2ccc(O)cc2)C(C)C)c1
HCID57933955

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C2CCc3cc(O)ccc3C2)c(N(Cc2ccc(OCCN(C)C)cc2)C(C)C)c1
HCID57934502

未命名化合物

收率 45.7%

PROCEDURE

实验过程

Synthesized from pivalic acid 6-{2-[(4-hydroxybenzoyl)isopropylamino]-4-methoxyphenyl}-5,6,7,8-tetrahydronaphthalen-2-yl ester (30 mg) and 2-chloro-N,N-dimethylacetamide (14 mg) according to an analogous synthetic method to Example 404 and purified by LC-MS, the title compound (13 mg) was obtained.

WORKUP

后处理

  1. custompurified by LC-MS