Hydroxylamine → HCID 86645281, compound

Participants

Reaction Steps

To a stirred solution of 8-bromo-5-isoquinolinecarboxaldehyde (i.e. a product from Step A) (75 mg, 0.3 mmol) in ethanol (7 mL) was added an aqueous solution of hydroxylamine (0.5 mL, 50% in water). After stirring at room temperature, overnight, the reaction mixture was concentrated under reduced pressure to provide the title compound as a yellow solid (70 mg).

Provenance & Evidence