HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Isopropylhydrazine → 5-amino-1-isopropyl-1H-pyrazole-4-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Isopropylhydrazine | HCID 52789 | — |
| Reactant | 5-amino-1-(2-methoxyphenyl)-1H-pyrazole-4-carbonitrile | HCID 12150560 | — |
| Product | 5-amino-1-isopropyl-1H-pyrazole-4-carbonitrile | HCID 17962028 | — |
Reaction Steps
Following the procedure for the preparation of 5-amino-1-(2-methoxyphenyl)-1H-pyrazole-4-carbonitrile but substituting 1-isopropylhydrazine provided the title compound. 400 MHz 1H NMR (CDCl3) δ 7.50 (s, 1H), 4.22-4.16 (m, 3H), 1.45 (d, J=6.6 Hz, 6H). MS: (M+H m/z=151.1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964607B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-6d314746dc2e448d8fed8f15a6b8e3f2 |
| Source note | uspto-grants-2011_06 |