HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Bromophenyl)boronic acid → HCID 67248034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Bromophenyl)boronic acid | HCID 79599 | — |
| Reactant | 5-Bromopyrimidine-2-carbonitrile | HCID 686546 | — |
| Reactant | 5-(4-Bromophenyl)picolinonitrile | HCID 58478022 | — |
| Product | HCID 67248034 | HCID 67248034 | 58% |
Reaction Steps
The same procedure described for 5-(4′-bromophenyl)-2-pyridinecarbonitrile was used by employing 5-bromo-2-cyanopyrimidine and 4-bromophenylboronic acid to furnish 84 in 58% yield; mp 202-204° C. 1H NMR (DMSO-d6): δ 7.79 (d, J=8.4 Hz, 2H), 7.88 (d, J=8.4 Hz, 1H), 9.39 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964619B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-9250df703c214230900e698219ca1c80 |
| Source note | uspto-grants-2011_06 |