HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → Ethyl 1-(pyridin-3-yl)cyclopropane-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | Ethyl 3-pyridylacetate | HCID 96490 | — |
| Product | Ethyl 1-(pyridin-3-yl)cyclopropane-1-carboxylate | HCID 21054369 | — |
Reaction Steps
Prepared in a similar manner to that described above by reacting ethyl 2-pyridin-3-ylacetate with 1,2-dibromoethane to give ethyl 1-pyridin-3-ylcyclopropane-1-carboxylate which was then hydrogenated to give the desired compound as a brown oil (quantitative reaction).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964618B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-05c0d4fc55d9412d928d375df8b38f21 |
| Source note | uspto-grants-2011_06 |