Hydrochloric Acid → HCID 59465583, compound

Participants

Reaction Steps

LiOH (1 mL, 1 mmol, 1 M) was added to a solution of 4 (43 mg, 0.10 mmol) in THF (5.5 mL). The mixture was stirred overnight and then 1 M HCl was added. The resulting mixture was extracted with dichloromethane (3×25 mL) and the combined organic solution was dried (Na2SO4), filtered and evaporated. Flash chromatography on silica gel (3% methanol/dichloromethane) gave 5 (41 mg, 100%).

Provenance & Evidence