Methyl iodide → HCID 11530076, compound

HRID 2425118Notes

Reaction equation

[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][NH:7][S:8]([C:11]1[CH:16]=[CH:15][C:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[CH:13][CH:12]=1)(=[O:10])=[O:9].[CH3:23]I>>[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][N:7]([CH3:23])[S:8]([C:11]1[CH:12]=[CH:13][C:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[CH:15][CH:16]=1)(=[O:10])=[O:9]

Participants

Reactant 2

HCID 6328Methyl iodide

HCID 11609430[1,1'-Biphenyl]-4-sulfonamide, N-(5-hydroxypentyl)-

Product 1

HCID 11530076HCID 11530076, compound

Procedure

Using a method analogous to that described in Example 4, with biphenyl-4-sulfonic acid-(5-hydroxypentyl)-amide and methyl iodide, the title compound was obtained. δC (CDCl3, 62.9 MHz): 22.7, 27.4, 32.2, 34.7, 50.0, 62.7, 127.4, 127.9, 128.5, 129.1, 136.0, 139.3 and 145.4.

Sources & evidence

ORD record: ord-9b82cfe833174fda84a3a2f7e190b498
Source dataset: uspto-grants-2011_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07964643B2

Reaction notes

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