1-Bromopentane → HCID 11501984, compound

HRID 2425120Notes

Reaction equation

HRID 2425120 reaction equation
[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][NH:7][S:8]([C:11]1[CH:16]=[CH:15][C:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[CH:13][CH:12]=1)(=[O:10])=[O:9].Br[CH2:24][CH2:25][CH2:26][CH2:27][CH3:28]>>[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][N:7]([CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])[S:8]([C:11]1[CH:12]=[CH:13][C:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[CH:15][CH:16]=1)(=[O:10])=[O:9]

Participants

3

Reactant 2

HCID 80571-BromopentaneHCID 11609430[1,1'-Biphenyl]-4-sulfonamide, N-(5-hydroxypentyl)-

Product 1

HCID 11501984HCID 11501984, compound

Procedure

Using a method analogous to that described in Example 4, with biphenyl-4-sulfonic acid-(5-hydroxypentyl)-amide and bromopentane, reacted at 60° C. for 3 hours, the title compound was obtained as an amorphous white solid. δC (CDCl3, 62.9 MHz): 14.0, 22.3, 22.9, 28.4, 28.6, 28.9, 32.2, 48.2, 48.4, 62.7, 127.3, 127.6, 128.4, 129.1, 138.6, 139.4 and 145.2.

Workup

  1. customreacted at 60° C. for 3 hours

Sources & evidence

ORD record
ord-ba6c9b14e03c4593ad72380ee1ff0b7a
Source dataset
uspto-grants-2011_06
Patent number
US07964643B2

Reaction notes

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