HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Toluene → HCID 18179455, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Toluene | HCID 1140 | — |
| Edukt | Dimethylformamide | HCID 6228 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 4'-Fluorobiphenyl sulfonic acid | HCID 18179513 | — |
| Produkt | HCID 18179455 | HCID 18179455 | — |
Reaktionsschritte
4′-Fluorobiphenyl sulfonic acid (3 g) was refluxed in thionyl chloride (30 mL) with a catalytic quantity of DMF (0.5 mL) for 4 hours. Toluene was added and the solvents evaporated under vacuum to give the title compound as an amorphous solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07964643B2 |
| Quelldatensatz | uspto-grants-2011_06 |
| ORD ID | ord-9c4a67b14b954527a80f0abf8b367bc8 |
| Quellennotiz | uspto-grants-2011_06 |