Tolylboronic acid → [1,1'-Biphenyl]-4-sulfonamide, N-(5-hydroxypentyl)-4'-methyl-

Participants

Role	Name	HCID	Charge
Reactant	Tolylboronic acid	HCID 79799	—
Reactant	4-Bromo-N-(5-hydroxypentyl)benzene-1-sulfonamide	HCID 16094721	—
Product	[1,1'-Biphenyl]-4-sulfonamide, N-(5-hydroxypentyl)-4'-methyl-	HCID 11508246	—

Reaction Steps

Using a method analogous to that described in Example 40, 4-bromophenyl-sulfonic acid-(5-hydroxypentyl)-amide and 4-methylphenyl boronic acid were reacted to give the title compound as a white solid. δC (DMSO, 62.9 MHz): 20.8, 22.6, 28.9, 32.0, 42.6, 60.5, 126.9, 127.0, 127.3, 129.7, 135.7, 138.0, 139.0 and 143.7.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07964643B2
Source dataset	uspto-grants-2011_06
ORD ID	ord-442f6ef32f33489c8bfd6da1ad3cecf5
Source note	uspto-grants-2011_06