HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetylphenylboronic acid → 4'-Acetyl-N-(5-hydroxypentyl)[1,1'-biphenyl]-4-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetylphenylboronic acid | HCID 3702122 | — |
| Reactant | 4-Bromo-N-(5-hydroxypentyl)benzene-1-sulfonamide | HCID 16094721 | — |
| Product | 4'-Acetyl-N-(5-hydroxypentyl)[1,1'-biphenyl]-4-sulfonamide | HCID 16094733 | — |
Reaction Steps
Using a method analogous to that described in Example 40, 4-bromophenyl-sulfonic acid-(5-hydroxypentyl)-amide and 4-acetylphenyl boronic acid were reacted to give the title compound as a white solid. δC (DMSO, 62.9 MHz): 22.6, 26.9, 28.9, 32.0, 42.6, 60.5, 127.0, 127.3, 127.9, 128.9, 136.4, 140.2, 142.5, 142.9 and 197.6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964643B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-8c0a1ce78ef4481cb1323fc36aadfa06 |
| Source note | uspto-grants-2011_06 |