4-Cyanophenylboronic acid → [1,1'-Biphenyl]-4-sulfonamide, 4'-cyano-N-(5-hydroxypentyl)-

Participants

Reaction Steps

Using a method analogous to that described in Example 40, 4-bromophenyl-sulfonic acid-(5-hydroxypentyl)-amide and 4-cyanophenyl boronic acid were reacted to give the title compound as a white solid. δC (DMSO, 62.9 MHz): 22.6, 28.9, 32.0, 42.6, 60.5, 111.0, 118.7, 127.3 127.0, 127.9, 128.1, 133.0, 140.6, 141.9 and 143.1.

Provenance & Evidence