HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyphenylboronic acid → [1,1'-Biphenyl]-4-sulfonamide, N-(5-hydroxypentyl)-2'-methoxy-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyphenylboronic acid | HCID 2733958 | — |
| Reactant | 4-Bromo-N-(5-hydroxypentyl)benzene-1-sulfonamide | HCID 16094721 | — |
| Product | [1,1'-Biphenyl]-4-sulfonamide, N-(5-hydroxypentyl)-2'-methoxy- | HCID 11530388 | — |
Reaction Steps
Using a method analogous to that described in Example 40, 4-bromophenyl-sulfonic acid-(5-hydroxypentyl)-amide and 2-methoxyphenyl boronic acid were reacted to give the title compound as a clear oil. δC (DMSO, 62.9 MHz): 22.7, 29.0, 32.0, 42.7, 55.6, 60.6, 115.5, 121.4, 125.3, 126.1, 128.2, 129.8, 130.2, 138.8, 142.1 and 156.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964643B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-61367b5932e74719b5cc400242f5d719 |
| Source note | uspto-grants-2011_06 |