HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxyphenylboronic acid → [1,1'-Biphenyl]-4-sulfonamide, 4'-hydroxy-N-(5-hydroxypentyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxyphenylboronic acid | HCID 2734360 | — |
| Reactant | 4-Bromo-N-(5-hydroxypentyl)benzene-1-sulfonamide | HCID 16094721 | — |
| Product | [1,1'-Biphenyl]-4-sulfonamide, 4'-hydroxy-N-(5-hydroxypentyl)- | HCID 11559081 | — |
Reaction Steps
Using a method analogous to that described in Example 40, 4-bromophenyl-sulfonic acid-(5-hydroxypentyl)-amide and 4-hydroxyphenyl boronic acid were reacted to give the title compound as a white solid. δC (DMSO, 62.9 MHz): 22.6, 28.9, 32.0, 42.6, 60.5, 116.0, 126.4, 127.2, 128.2, 129.2, 138.1, 143.8 and 158.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964643B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-7b7257ee2c604279bb48aa47308ec2aa |
| Source note | uspto-grants-2011_06 |