3-Tolylboronic acid → [1,1'-Biphenyl]-4-sulfonamide, N-(4-hydroxybutyl)-3'-methyl-

Participants

Role	Name	HCID	Charge
Reactant	3-Tolylboronic acid	HCID 2733950	—
Reactant	4-Bromo-N-(4-hydroxybutyl)benzene-1-sulfonamide	HCID 16094720	—
Product	[1,1'-Biphenyl]-4-sulfonamide, N-(4-hydroxybutyl)-3'-methyl-	HCID 11609431	—

Reaction Steps

Using a method analogous to that described in Example 40, 4-bromophenyl-sulfonic acid-(4-hydroxybutyl)-amide and 3-methylphenyl boronic acid were reacted to give the title compound as a white solid. δC (DMSO, 62.9 MHz): 21.1, 25.8, 29.5, 42.6, 60.2, 124.1, 127.1, 127.3, 129.0, 138.4, 138.6, 139.2 and 143.9.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07964643B2
Source dataset	uspto-grants-2011_06
ORD ID	ord-e719b94fe883473498027a4f8283f45b
Source note	uspto-grants-2011_06