Methyl iodide → HCID 11696728, compound

HRID 2425170Notes

Reaction equation

[OH:1][CH:2](C)[CH2:3][CH2:4][CH2:5][NH:6][S:7]([C:10]1[CH:15]=[CH:14][C:13]([C:16]2[CH:21]=[CH:20][C:19]([C:22]([F:25])([F:24])[F:23])=[CH:18][CH:17]=2)=[CH:12][CH:11]=1)(=[O:9])=[O:8].[CH3:27]I>>[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][N:6]([CH3:27])[S:7]([C:10]1[CH:11]=[CH:12][C:13]([C:16]2[CH:17]=[CH:18][C:19]([C:22]([F:25])([F:24])[F:23])=[CH:20][CH:21]=2)=[CH:14][CH:15]=1)(=[O:8])=[O:9]

Participants

Reactant 2

HCID 6328Methyl iodide

HCID 86620301HCID 86620301, compound

Product 1

HCID 11696728HCID 11696728, compound

Procedure

Using a method analogous to that described in Example 4, 4′-trifluoromethylbiphenyl-4-sulfonic acid-(4-hydroxypentyl)-amide and methyl iodide were reacted to give the title compound as a white solid.

Workup

customwere reacted

Sources & evidence

ORD record: ord-73c6974ca55244448e14a675cc75881d
Source dataset: uspto-grants-2011_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07964643B2

Reaction notes

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