Phenylpropionylglycine → HCID 59689164, compound

HRID 2425176Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([NH:15][CH3:16])[C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:4][CH:3]=1.[C:17]1([CH2:23][CH2:24][C:25]([NH:27][CH2:28][C:29]([OH:31])=O)=[O:26])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH:8]([N:15]([CH3:16])[C:29]([CH2:28][NH:27][C:25](=[O:26])[CH2:24][CH2:23][C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=2)=[O:31])[C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:6][CH:7]=1

Participants

Reactant 2

HCID 152323Phenylpropionylglycine

HCID 43389364HCID 43389364, compound

Product 1

HCID 59689164HCID 59689164, compound

Procedure

Prepared in analogy to example 1.1 from rac-[(4-chloro-phenyl)-phenyl-methyl]-methylamine (CA [118762-04-2]) and (3-phenyl-propionylamino)-acetic acid (CA [56613-60-6]).

Sources & evidence

ORD record: ord-86b1569124cb4712aa53f94dc5859192
Source dataset: uspto-grants-2011_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07964645B2

Reaction notes

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