5-Nitro-2-thenoic acid → HCID 24897001, compound

HRID 2425201Notes

Reaction equation

HRID 2425201 reaction equation
Cl.[NH2:2][CH2:3][C:4]([NH:6][CH:7]([C:14]1[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][CH:15]=1)[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:5].[N+:21]([C:24]1[S:28][C:27]([C:29](O)=[O:30])=[CH:26][CH:25]=1)([O-:23])=[O:22]>>[Cl:20][C:17]1[CH:18]=[CH:19][C:14]([CH:7]([NH:6][C:4]([CH2:3][NH:2][C:29]([C:27]2[S:28][C:24]([N+:21]([O-:23])=[O:22])=[CH:25][CH:26]=2)=[O:30])=[O:5])[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:15][CH:16]=1

Participants

3

Reactant 2

HCID 805915-Nitro-2-thenoic acidHCID 672464382-Amino-N-[(4-chloro-phenyl)-phenyl-methyl]-acetamide hydrochloride

Product 1

HCID 24897001HCID 24897001, compound

Procedure

Prepared in analogy to example 1.12 from rac-2-amino-N-[(4-chloro-phenyl)-phenyl-methyl]-acetamide hydrochloride (Example 3.1) and 5-nitrothiophene-2-carboxylic acid. MS (m/e): 428.3 (MH−, 100%).

Sources & evidence

ORD record
ord-eb192183090b4726ad761eb5e102458f
Source dataset
uspto-grants-2011_06
Patent number
US07964645B2

Reaction notes

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