Chloroacetyl chloride → HCID 67245794, compound

HRID 2425595Notes

Reaction equation

C(O[C:6]([N:8]1[CH2:14][CH2:13][CH2:12][NH:11][CH2:10][CH2:9]1)=O)(C)(C)C.[Cl:15]C[C:17](Cl)=[O:18].[NH:20]1[CH2:25][CH2:24][O:23][CH2:22][CH2:21]1>>[ClH:15].[ClH:15].[N:8]1([CH2:6][C:17]([N:20]2[CH2:25][CH2:24][O:23][CH2:22][CH2:21]2)=[O:18])[CH2:14][CH2:13][CH2:12][NH:11][CH2:10][CH2:9]1

Participants

Reactant 3

HCID 6577Chloroacetyl chloride

HCID 8083Morpholine

HCID 2756058Tert-butyl 1,4-diazepane-1-carboxylate

Product 1

HCID 67245794HCID 67245794, compound

Procedure

prepared from [1,4]diazepane-1-carboxylic acid tert-butyl ester, chloroacetylchloride and morpholine in an analogous manner as described in example 15.

Sources & evidence

ORD record: ord-947e5062eb944095a7ea289528616ea8
Source dataset: uspto-grants-2011_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07964724B2

Reaction notes

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