HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Diazepan-5-one → HCID 67012877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Diazepan-5-one | HCID 2737264 | — |
| Reactant | HCID 86602322 | HCID 86602322 | — |
| Product | HCID 67012877 | HCID 67012877 | — |
Reaction Steps
1-[(4S,5R)-2-(4-tert-Butyl-2,5-diethoxy-phenyl)-4,5-bis-(4-chloro-phenyl)-4,5-dihydro-imidazole-1-carbonyl]-[1,4]diazepan-5-one hydrochloride was prepared from (4S,5R)-2-(4-tert-butyl-2,5-diethoxy-phenyl)-4,5-bis-(4-chloro-phenyl)-4,5-dihydro-imidazole-1-carbonyl chloride (example 12f) and [1,4]diazepan-5-one (Oakwood Products) in an analogous manner as described in example 25. LR-MS: 651.4 [(M+H)+]
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964724B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-a6b6a0fe6e8f416e8d255791f43eb562 |
| Source note | uspto-grants-2011_06 |