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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2425729Generated: November 2, 2026

2-Methylimidazole → HCID 67246581, compound

https://huagongshe.com/reaction/2425729

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MethylimidazoleHCID 12749—
ReactantValeryl chlorideHCID 61186—
ReactantHCID 23726674HCID 23726674—
ProductHCID 67246581HCID 6724658177.7%

Reaction Steps

In a manner similar to Example 5 and starting from 15 g (62 mmol) of N-(4-chlorobenzyl)-L-Valine, 12 mL (99 mmol) of valeryl chloride and 7.7 g (93 mmol) of 2-methylimidazole, 15.7 g (77%) of N-(4-chlorobenzyl)-N-valeryl-L-Valine is obtained. The solid is recrystallised from a mixture of EtOH:H2O 1:1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07964749B2
Source datasetuspto-grants-2011_06
ORD IDord-c3792ce4272b4b4e8c174b20fdb92ff9
Source noteuspto-grants-2011_06