HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylimidazole → HCID 67246581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylimidazole | HCID 12749 | — |
| Reactant | Valeryl chloride | HCID 61186 | — |
| Reactant | HCID 23726674 | HCID 23726674 | — |
| Product | HCID 67246581 | HCID 67246581 | 77.7% |
Reaction Steps
In a manner similar to Example 5 and starting from 15 g (62 mmol) of N-(4-chlorobenzyl)-L-Valine, 12 mL (99 mmol) of valeryl chloride and 7.7 g (93 mmol) of 2-methylimidazole, 15.7 g (77%) of N-(4-chlorobenzyl)-N-valeryl-L-Valine is obtained. The solid is recrystallised from a mixture of EtOH:H2O 1:1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964749B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-c3792ce4272b4b4e8c174b20fdb92ff9 |
| Source note | uspto-grants-2011_06 |