HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 59128274, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Ethoxy-4-methylbenzaldehyde | HCID 25242058 | — |
| Reactant | HCID 86607633 | HCID 86607633 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 59128274 | HCID 59128274 | — |
Reaction Steps
The title compound was prepared analogously to 3-ethoxy-4-methyl-benzaldehyde (intermediate D10, vide infra) by reaction of 2-chloro-3,5-dihydroxy benzaldehyde with iodoethane in DMF using K2CO3 as base. MS (ISP): 229.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968568B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-37dd7f323359477489b402ab7104324a |
| Source note | uspto-grants-2011_06 |